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3Flex Chemisorption Option- High Resolution, High-throughput Surface Characterization Analyzer
With the chemisorption option, the 3Flex is configured to perform chemical adsorption analyses that enable the researcher to obtain valuable information about the physical or chemical properties of catalysts, catalyst supports, and a variety of other materials.
3Flex TCD Dynamic Chemisorption option High Resolution, High-throughput Surface Characterization Analyzer
Perform High Resolution TPR, TPO, and TPD Experiments Micromeritics 3Flex, the industry’s most highly recognized and preferred instrument for physisorption and chemisorption1, has been made even more powerful.
ASAP2020 Plus Chemisorption Option -Accelerated Surface area & Porosimetry System
The ASAP 2020 Plus Chemisorption option permits you to obtain valuable information about the physical and chemical properties of your catalyst, catalyst support, adsorbents, and other materials. Its unique design provides a high level of system cleanliness to permit low-pressure chemisorption isotherms.
AutoChem II 2920 Automated Catalyst Characterization System
Automated Catalyst Characterization System – A catalyst characterization laboratory enclosed in one cabinet.
The AutoChem II 2920 is a fully automated chemisorption analyzer that can provide your laboratory with the ability to conduct a comprehensive array of highly precise studies of chemical adsorption and temperature-programmed reactions.
Superior Performance Under Extended Pressure
Micromeritics’ AutoChem 2950 HP Chemisorption Analyzer is an automated high-pressure catalyst characterization system that is capable of preparing and analyzing samples at elevated pressures up to 1000 psia and at temperatures from -100 to 1100 °C. The instrument can perform a variety of experiments including pulse chemisorption, BET surface area, temperature-programmed reduction (TPR), desorption (TPD), oxidation (TPO), and reaction analyses.
The ChemiSorb 2720 and ChemiSorb 2750 can be equipped to perform chemical and physical adsorption tests that are central to the development, testing, and production of catalysts. They employ the dynamic (flowing gas) technique of analysis by which the quantity of gas taken up by the sample or released from the sample surface is monitored by a Thermal Conductivity Detector (TCD). Data obtained by the instruments can be used to calculate key parameters for catalyst characterization: metal dispersion, active surface area, BET surface area, average crystallite size, surface acidity or basicity, and activation energy via first order kinetic models.
Optimum design and efficient utilization of catalysts require a thorough understanding of the surface structure and surface chemistry of the catalytic material. Chemical adsorption analyses can provide much of the information needed to evaluate catalyst materials in the design and production phases, as well as after a period of use.
This “Owner Configured” Computerized and automatic pilot plant is based on a CSTR (from 100cc up to 4L and many different alternatives) and the operation is supported by many optional devices as MFC´s, pumps, pre-heaters, separators, pressure control systems. Customer can design his own pilot plant using for it so many options as required for his operation needed, using for it a configuration sheet.
Fixed Bed Reactor
The PID/Particulate Systems Effi Microreactor, is a highly-advanced modular laboratory system for measuring the activity and selectivity of catalysts. The Effi Microreactor has been developed to help save time and resources at both the catalyst development stage and the factory report process during the screening.
It can accommodate a wide variety of reactions including hydrocracking, hydrotreating, isomerization, hydrogenation, hydrodesulphurization (HDS), oxidation, hydrodenitrogenation (HDN), reforming (aromatization), GTL (Fischer-Tropsch), and steam reforming, to name a few.
This unit is a fully automatic and computerized laboratory reactor (described in ES2011993 patent) for the analysis of Fluid Cracking Catalysts (FCC). This MAT reactor is design to perform up to four independent and consecutive FCC test, following the norms described by the standard method ASTM D3907, in automatic mode without the presence of an operator.
Due to the renewed interest on innovative ways to convert the existing fuel reserves with improved technologies like gasification, PID Eng&Tech has worked in collaboration with important researches in the field of gasification in order to develop the most versatile pilot plant existing in the market nowadays. Its versatility and complete automatization, allows the user to determine optimal experimental conditions and detecting possible operational problem in industrial gasifiers.
The Micromeritics in-situ Catalyst Characterization System (ICCS) is an advanced catalyst characterization tool that allows the user to study the impact of a reaction on critical parameters such as number of active sites, under precisely controlled, process-representative conditions.
A standalone accessory designed to complement any dynamic laboratory reactor system, such as the MicroActivitySystems, the ICCS adds two new capabilities: Temperature Programmed Analyses (TPx) and Pulse Chemisorption.
The Polymerization Micro-Pilot Plant, developed by PID Eng&Tech , is designed for continuous production at microscale.
PID Eng&Tech in co-operation with important Research and Technology Centres by means of different Collaboration Projects has developed a pilot plant to produce polyolefins. The plant comprises two continuous stirred-tank reactors that operate in series.
The Selective Adsorption Analyzer SAA 8100 is a gas delivery system based upon the technology of PID Engineering and Technology, a Micromeritics company. The primary components of the system include mass flow controllers, blending valves, vapor sources, temperature control, and a simple column for evaluating adsorbents. The basic procedure for evaluating an adsorbent candidate includes: activation (degassing) of the adsorbent, flow a mixture of gases (or vapors) through the column containing the adsorbent, and monitor the composition of the effluent gas from the column containing the adsorbent.
Improving competitiveness in the industry is sharply marked by developing new products with high quality features and a high added value. Continuous and automatic pilot plants that can simulate industrial processes at the laboratory level with reasonable scalability are essential for seeking new products, improving the quality of existing ones and developing new processes.