Breakthrough Analyzer (BTA)

A Compact, Versatile, High-Performance Selective Adsorption System.

  • Superior design minimizes dead volume & delivers accurate, experimental results
  • Configurable with up to 6 precision mass flow controllers and 2 vapor sources
  • Patented high-performance blending valves
  • Sample activation up to 1050℃
  • Thermostated environmental chamber provides uniform temperature control, even when using vapors
  • Easily connects to commercial Mass Spectrometer (MS) & Fourier Transform Infrared Analyzer (FTIR)
  • Secure door lock system for enhanced operator safety

Description

Engineered for Performance

The new BreakThrough Analyzer (BTA) is a flexible gas delivery and management system for the precise characterization of adsorbent performance under process-relevant conditions. It delivers reliable adsorption data for gas/vapor mixtures using a flow-through system.

A safe and highly optimized device for collecting both transient and equilibrium adsorption data for multi component systems. The BTA can be configured with up to six precision mass flow controllers and patented high performance blending valves, delivering unparalleled flexibility in experimental design. The superior gas-delivery design ensures the precise control of both composition and flow rate, while minimizing dead volume.

The high-quality, stainless-steel column can hold 0.05 to 2.5 grams of adsorbent. Automated sample activation up to 1050°C is possible with the precise, rugged, and reliable resistance furnace.

Operating pressures are controlled from atmospheric to 30 bar via a servo positioned controlled valve. The thermostated environmental chamber delivers uniform temperature control of the entire system up to 200°C, eliminating cold spots. The BTA secure door lock system ensures operator safety throughout the analysis.

Vapor generators can be added to the BTA to enable the use of important probe molecules such as water for experimental studies. The BTA easily connects to commercially available Fourier Transform Infrared and Mass Spectrometer systems for gas identification and quantification.

Key Features

  • Fully configurable to the user’s catalytic testing needs with a variety of configurations and options
  • Small footprint saves expensive lab space and optionally allows installation within a fume hood
  • Automated routines minimize user errors and reduce test time
  • Equipped with embedded control featuring multiple temperature and pressure sensors for monitoring and controlling reaction studies
  • Expandable for future needs, e.g. detectors or optional accessories (e.g. GC/MS, additional gas and liquid feeds, Liquid Liquid Gas (LLG) separator, others upon request) that protects your investment
  • Integrated safety system can be used in automatic and autonomous mode to protect lab staff and instrument. The safety system ensures that both, the user and the instrument is protected.
  • Pressure control to perform experiments at commercially relevant conditions

Configurable Activity and Selectivity Testing in a Small Footprint

Key Features:

  • Customizable to the user’s catalytic testing needs with a variety of configurations and options
  • Small footprint saves expensive lab space and optionally allows installation within a fume hood
  • Automated routines minimize user errors and reduce test time – and can be monitored remotely
  • Equipped with embedded control featuring multiple temperature and pressure sensors for monitoring and controlling reaction studies
  • Expandable for future needs, eg. detectors or optional accessories (e.g. GC/MS, additional gas and liquid feeds.
  • Liquid-Liquid Gas (LLG) separator, upon request) that protects your investment
  • Integrated safety system can be used in automatic and autonomous mode to protect lab staff a and unit
  • Pressure control to perform experiments at commercially relevant conditions

With regard to measuring catalytic activity and selectivity, catalyst screening, study of operation conditions, reaction kinetic and reaction-regeneration cycles, the Micromeritics FR series features three models:

  • Micromeritics Flow Reactor FR 50: Compact basic semi-automated catalyst testing unit, upgradable standard options at any time.
  • Micromeritics Flow Reactor FR 100: Advanced modular and fully automated laboratory system, upgradable with standard and customized non-standard options.
  • Micromeritics Flow Reactor FR 200: Dual-reactor system that may be configured to perform reaction studies in series or parallel.

A safe and highly optimized device for collecting both transient
and equilibrium adsorption data for multi-component systems.

  • Shut off from the software
  • Door closed during the analysis
  • Furnace temperature control alarm
  • Thermostated environmental chamber temperature control alarm
  • Optional connection to shut off system
  • Optional valve to shut off all MFC’s
  • Optional gas detector in the thermostated environmental chamber
  • Optional valve shut off valve

Additional Specs

  • Determination of breakthrough curves
  • Investigation of kinetic performance of adsorbents
  • Investigation of co-adsorption and displacement
  • Determination of sorption selectivity
  • High-resolution separations using small sample quantities
  • Dynamic adsorption and desorption experiments
  • Determination of single- and multi-component adsorption data
  • In-situ sample preparation up to 450°C with a SS column and 1050°C with a quartz column
  • Fully automated control via PC
  • Up to 6 high precision mass flow controllers
  • Programmable total pressure, flow rate, composition and temperature
  • Optimised for research-scale sample sizes with interchangeable reactor beds
  • Ultra-low dead volume for rapid signal response
  • Automated switching between purge and process gases
  • Configurations for gas-vapor and vapor-vapor separation
  • Door remains locked during analysis to protect user and the analysis from altered temperature conditions
  • Touch Screen
  • Patented “No Dead Volume” mixing valve with rapid switching

Documents

BTA Brochure

Video