Saturn DigiSizer II

Micromeritics

Overview – Saturn DigiSizer II High-Definition Digital Particle Size Analyzer

 Major Advance in Particle Sizing Technology

The Saturn DigiSizer®II  is the first commercially available particle sizing instrument to employ the light scattering analysis technique that utilizes advanced digital detection technology to deliver exceptionally high levels of resolution, accuracy, repeatability, and reproducibility. A state-of-the-art CCD detector containing over three million detector elements enables the completely automated Saturn DigiSizer II to capture a high resolution, digital representation of the pattern produced as a result of laser light scattered from a sample. The resulting information is then processed using data reduction based on Mie theory. The instrument produces fast, detailed results that are repeatable on and reproducible between every Saturn DigiSizer.

Particle sizing techniques have advanced significantly throughout the past several decades. One of the most important contributions to this field is the application of laser-based technologies, complemented with the use of modern photo-detectors and digital computers. For some time, progress in laser light scattering technology has led to faster analyses, but the quality of the measurement was limited, often due to inadequacies in the detector.
Recognizing this need for better detection capability, Micromeritics developed the Saturn DigiSizer, an instrument that employed a laser diode and modern charge-coupled device (CCD) detector to significantly improve the sensitivity, resolution, reproducibility, and repeatability of the laser light scattering particle sizing technique.



 

Features

Sensitivity, High Resolution, Reproducibility, Repeatability

With the Saturn DigiSizer II, Micromeritics has again improved this particle size technique. Utilizing a state-of-the-art CCD detector containing over three million detector elements, Mie theory, and unique design and data reduction features, the Saturn DigiSizer II gives users an extremely high level of resolution and sensitivity not available in other laser particle sizing systems. The level of detail, accuracy, and resolution enables the extraction of all available information from the static light scattering pattern. Users can now measure the same material on multiple instruments located at different locations around the world and get the same, highly detailed size distribution measurement on each instrument. The Saturn DigiSizer II is fully automated and requires little operator intervention.

  • Measures both organic and inorganic particles ranging from 40 nanometers to 2.5 millimeters equivalent spherical diameter.
  • CDC detector contains over three million detector elements producing extremely high-resolution data.
  • Adjustable liquid sample handling unit for automatic sampling, dilution, and dispersion is available in both standard and low-volume configurations.
  • One computer can control up to two Saturn DigiSizers each with a liquid sample handling unit.
  • Optional MasterTech 052 Autosampler provides unattended analysis of up to 18 samples.
  • Fast, detailed results are repeatable on, and reproducible between, every Saturn DigiSizer II.
  • User-friendly analysis program includes wizards and intuitive screens and is designed to operate in the Windows® environment
Advantages:✔ Superior sensitivity
✔ Higher resolution
✔ Superior analysis-to-analysis repeatability
✔ Greater accuracy
✔ Better reproducibility
✔ Exceptional data quality
✔ Fully automated system
✔ Versatile sample handling options
✔ Easy-to-use software
✔ 21 CFR Part 11 software option
✔ IQ/OQ validation service option
✔ No proprietary “black-box” algorithms

Pharmaceuticals – Particle size plays a major role in the ability to process, blend, tablet, and package a drug substance. The useful shelf life and dissolution rate (governing how rapidly the medicine becomes available to the body) depend upon the particle size of the material.

Ceramics – Particle Size information helps to determine curing and bonding procedures, control pore structure, ensure adequate green body strength, and produce a final product of desired strength, texture, appearance, and density.

Catalysts – Flow properties of fluid-cracking catalysts depend upon the particle size distribution of the particles. Surface area and pore structure of acid catalysts and catalyst supports result from the particle size distribution of the particles that are used to produce them.

Paints and Coatings – The particle size distribution of the pigment or filler influences the porosity, gloss, texture, color, color saturation, brightness, solids content, and film adhesion properties. The resulting porosity can control application properties such as fluidity, drying or setting time, and film thickness.

Cosmetics – The appearance, application, and packaging of cosmetics are influenced by the particle size distribution of the base powders, such as talc, and the pigments used in coloring.

Abrasives – Performance of abrasives, either in powder form or after being attached to a backing, is dictated by the size distribution of the abrasive powder. Over-sized particles lead to scratching and gouging. Undersized particles may lead to clogging of the abrasive papers.

Mining – Refining efficiency of materials is related strongly to the particle size distribution of the raw mineral. For products that are used without chemical change, the size of particles taken from the mine may be too large for final usage. Analyses performed on the extracted minerals will help determine the amount of size reduction needed once the product reaches the processing plant.

Column Packing Materials – The back-pressure of the packed bed within the column is a direct function of the size of the channels through the bed and, thus, the size distribution of the column packing material. Over-sized particles create voids in the bed, reducing efficiency due to remixing of the separated sample components. Undersized particles lead to blockage of flow paths through the bed, increasing the back-pressure and analysis time. A proper distribution leads to greater separation efficiency.

Superior Data Reduction and Reporting

The Saturn DigiSizer II’s powerful, easy-to-use and versatile user interface provides all the convenient features you expect from a Windows-based program such as point-and-click menus, multitasking capability, copy to clipboard, and more. The familiar Windows format reduces the time required for training and eliminates the need for most off-line data manipulation, resulting in increased productivity. The analysis program is designed to operate in the Windows environment and includes wizards and intuitive screens enabling you to perform system operations quickly and efficiently.

In addition, Micromeritics’ confirm™ 21 CFR Part 11 software assists with compliance to FDA regulations. Combined with Micromeritics’ IQ and OQ services, the user can be assured that the Saturn DigiSizer II system is validated for accuracy, reliability, consistent performance, and provides safeguards to protect the integrity of analysis records. System access is limited to authorized individuals. Secure, computer-generated, time-stamped audit trails are integral parts of the software program.

Wide Range of Data Presentation Options With many instruments that employ the static light scattering technique, a final report of reduced data typically is the only output available. The Saturn DigiSizer II, however, allows you to access the raw data. For instance, an image of the scattering pattern (2-D and 3-D representations) can be displayed, or you can receive a 592-point intensity versus angle data report in tabular or graphical form. To allow a quick assessment of the fit of theoretical models to experimental data, you also can obtain an overlay plot of measured data calculated from Mie theory.

Reduction of Raw Data Based on Mie Theory Ensures Exceptional Data Quality

Micromeritics employs the Mie theory (or the operator can choose to use Fraunhofer for particles that are both large and opaque) to reduce experimental data using a well-published, non-negative least squares method. These theories describe light scattering via theoretical models. No modifications to the theory are made with the Saturn DigiSizer II, and no assumptions of modality or distribution type are used. This is made possible by the remarkably high resolution of the optical system allowing very narrow size classes to be used in fitting the data to Mie theory.

The application of Mie theory provides unambiguous size data. In addition to reporting the data, the Saturn DigiSizer II can generate a plot that shows how well experimental measurements compare with theoretical Mie calculations for the scattering pattern from the reported distribution.

 

 

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